Type of feed | Concentration (mg/kg) |
---|---|
Wheat (n=3) | 0.05–0.08 |
Barley (n=3) | <LOQ |
Triticale (n=3) | <LOQ |
Ground paprika (n=3) | 0.58–1.87 |
Young corn (n=3) | 5.30–12.8 |
Fully grown corn (n=3) | 0.13–1.01 |
Compound feed (n=50) | <LOQ–0.48 |
Validation parameter | Material | ||||
---|---|---|---|---|---|
Corn | Compound feed | ||||
Linearity (R2) | 0.9936 | 0.9911 | |||
Limit of detection, LOD (mg/kg) | 0.05 | 0.02 | |||
Limit of quantification, LOQ (mg/kg) | 0.1 | 0.05 | |||
Concentration (mg/kg) | 0.25 | 0.5 1.0 | 0.25 | 0.5 | 1.0 |
Repeatability, CV (%) | 8.74 | 7.21 6.93 | 7.28 | 11.3 | 8.06 |
Reproducibility, CV (%) | 9.63 | 11.8 7.46 | 8.15 | 14.7 | 9.35 |
Recovery (%) | 101 | 98.3 97.8 | 105 | 100 | 95.3 |