<abstract xml:lang="en" xmlns="http://www.w3.org/1999/xhtml"><p>A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis, elemental analysis and IR spectroscopy. The single crystal X-Ray analysis shows that this polymer is 2-D along a axis. Flower-like nanostructure thallium (III) oxide, Tl2O3 has been prepared by direct thermal decomposition of thallium (I) coordination polymer. The nanostructure was characterized by scanning electron microscopy (SEM), X-Ray powder diffraction (XRD) and IR spectroscopy. The thermal stability of the Tl2O3 nanostructure was studied by thermal gravimetric analysis and differential thermal analysis (TGA /DTA) too.</p></abstract>

A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis, elemental analysis and IR spectroscopy. The single crystal X-Ray analysis shows that this polymer is 2-D along a axis. Flower-like nanostructure thallium (III) oxide, Tl2O3 has been prepared by direct thermal decomposition of thallium (I) coordination polymer. The nanostructure was characterized by scanning electron microscopy (SEM), X-Ray powder diffraction (XRD) and IR spectroscopy. The thermal stability of the Tl2O3 nanostructure was studied by thermal gravimetric analysis and differential thermal analysis (TGA /DTA) too.

Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Departement of Chemistry, Firoozabad Branch, Islamic Azad University, Firoozabad, Fars, Iran, P.O. Box 74715-117

Materials Science-Poland

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

A new thallium (I) coordination polymer [Tl(PsucH)]n (PsucH = phenylsuccinic acid) has been synthesized and characterized by single crystal X-Ray analysis,...

Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Publié en ligne: 26 mars 2014

Pages: 23 - 27

DOI: https://doi.org/10.2478/s13536-013-0151-3

Mots clés
thallium (I), coordination polymer, nanostructure, thallium (III) oxide

© 2014 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Thallium I phenylsuccinic acid coordination polymer as precursor for preparation of thallium (III) oxide nano structures by direct thermal decomposition

Publié en ligne: 26 mars 2014

Pages: 23 - 27

DOI: https://doi.org/10.2478/s13536-013-0151-3

Mots clésthallium (I), coordination polymer, nanostructure, thallium (III) oxide

© 2014 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Mots clés
thallium (I), coordination polymer, nanostructure, thallium (III) oxide