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<p>The tetracalcium phosphate/nanomonetite (TTCPMH) biocements with the addition of sodium alginate were prepared by mechanical homogenization of powder mixture with hardening liquid containing sodium alginate. The effect of various viscosity of different alginates on properties of TTCPMH cement mixture was investigated. The medium viscous (MED) alginate had a more negative effect on setting process and compressive strength than low viscous (LOW) alginate. An approx. 50% decrease in mechanical properties (compressive strengths, Young´s modulus, work of fracture (WOF)) was revealed after an addition of 0.25 wt % with rapid fall above 1 wt % of LOW alginate in biocement. A statistically significant difference in the WOF was found between of 0.25 and 0.5 LOW alginate biocements (p&lt;0.035) whereas no statistical differences were revealed between WOF of 0.5 and 1 LOW alginate biocements (p˃0.357). In the microstructure of composite cements, the increased amounts of granular or finer needle-like nanohydroxyapatite particles arranged into the form of more separated spherical agglomerates were observed. A low cytotoxicity of cement extracts based on measurement of cell proliferation was revealed.</p>
</abstract>

The tetracalcium phosphate/nanomonetite (TTCPMH) biocements with the addition of sodium alginate were prepared by mechanical homogenization of powder mixture with hardening liquid containing sodium alginate. The effect of various viscosity of different alginates on properties of TTCPMH cement mixture was investigated. The medium viscous (MED) alginate had a more negative effect on setting process and compressive strength than low viscous (LOW) alginate. An approx. 50% decrease in mechanical properties (compressive strengths, Young´s modulus, work of fracture (WOF)) was revealed after an addition of 0.25 wt % with rapid fall above 1 wt % of LOW alginate in biocement. A statistically significant difference in the WOF was found between of 0.25 and 0.5 LOW alginate biocements (p<0.035) whereas no statistical differences were revealed between WOF of 0.5 and 1 LOW alginate biocements (p˃0.357). In the microstructure of composite cements, the increased amounts of granular or finer needle-like nanohydroxyapatite particles arranged into the form of more separated spherical agglomerates were observed. A low cytotoxicity of cement extracts based on measurement of cell proliferation was revealed.

Influence of Sodium Alginate on Properties of Tetracalcium Phosphate/Nanomonetite Biocement

Powder Metallurgy Progress

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

The tetracalcium phosphate/nanomonetite (TTCPMH) biocements with the addition of sodium alginate were prepared by mechanical homogenization of powder mixture...

Influence of Sodium Alginate on Properties of Tetracalcium Phosphate/Nanomonetite Biocement

Publié en ligne: 15 juin 2020

Pages: 1 - 11

DOI: https://doi.org/10.1515/pmp-2019-0001

Mots clés
polymeric additive (sodium alginate), tetracalcium phosphate/nanomonetite biocement, mechanical properties, composites, bioactivity

© 2019 R. Štulajterová et al., published by Sciendo

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Influence of Sodium Alginate on Properties of Tetracalcium Phosphate/Nanomonetite Biocement

Publié en ligne: 15 juin 2020

Pages: 1 - 11

DOI: https://doi.org/10.1515/pmp-2019-0001

Mots cléspolymeric additive (sodium alginate), tetracalcium phosphate/nanomonetite biocement, mechanical properties, composites, bioactivity

© 2019 R. Štulajterová et al., published by Sciendo

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Mots clés
polymeric additive (sodium alginate), tetracalcium phosphate/nanomonetite biocement, mechanical properties, composites, bioactivity