<abstract xml:lang="en" xmlns="http://www.w3.org/1999/xhtml"><p>In order to overcome limitations in the processing parameters of powder compaction method, a novel processing technique based on sol-gel route has been developed to produce near-net-shaped prototype fine zirconia minispheres with required properties that could potentially be used as grinding media. Impact of magnesia concentration and sintering temperature on the final product has been analyzed in detail. Zirconia minispheres have been characterized to establish a correlation between physical, structural and mechanical properties. Sintering temperature, soaking period, heating rate and viscosity of the sol apparently influence the characteristics of the magnesia stabilized zirconia minispheres. The phase identification, density variation, chemical decomposition, functional group specification, surface area, porosity, shrinkage and microstructural features of the dried and sintered final product have been studied. It has been observed that magnesia content, sintering temperature, density and the grain size of the sintered minispheres have a significant impact on the mechanical properties of the final product.</p></abstract>

In order to overcome limitations in the processing parameters of powder compaction method, a novel processing technique based on sol-gel route has been developed to produce near-net-shaped prototype fine zirconia minispheres with required properties that could potentially be used as grinding media. Impact of magnesia concentration and sintering temperature on the final product has been analyzed in detail. Zirconia minispheres have been characterized to establish a correlation between physical, structural and mechanical properties. Sintering temperature, soaking period, heating rate and viscosity of the sol apparently influence the characteristics of the magnesia stabilized zirconia minispheres. The phase identification, density variation, chemical decomposition, functional group specification, surface area, porosity, shrinkage and microstructural features of the dried and sintered final product have been studied. It has been observed that magnesia content, sintering temperature, density and the grain size of the sintered minispheres have a significant impact on the mechanical properties of the final product.

Study on process development and property evaluation of sol-gel derived magnesia stabilized zirconia minispheres

Department of Physics, University VOC college of Engg., Anna University, Tuticorin, 628008, India

Department of Ceramic Technology, Anna University, Chennai, 600025, India

Materials Science-Poland

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

In order to overcome limitations in the processing parameters of powder compaction method, a novel processing technique based on sol-gel route has been...

Study on process development and property evaluation of sol-gel derived magnesia stabilized zirconia minispheres

Published Online: Jul 22, 2014

Page range: 145 - 156

DOI: https://doi.org/10.2478/s13536-013-0190-9

Keywords
zirconia minispheres, sol-gel synthesis, zirconium oxalate sol, magnesia stabilization

© 2014 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Study on process development and property evaluation of sol-gel derived magnesia stabilized zirconia minispheres

Published Online: Jul 22, 2014

Page range: 145 - 156

DOI: https://doi.org/10.2478/s13536-013-0190-9

Keywordszirconia minispheres, sol-gel synthesis, zirconium oxalate sol, magnesia stabilization

© 2014 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Keywords
zirconia minispheres, sol-gel synthesis, zirconium oxalate sol, magnesia stabilization