<abstract xml:lang="en" xmlns="http://www.w3.org/1999/xhtml"><p>In an effort to synthesize doped ZnO nanowires, SiOx nanowires were obtained accidently. In the experiment, mixed powders containing chemicals such as ZnO, graphite, Ga2O3, and In2O3 were placed in the center of a tube furnace, where the temperature was set to 1200 °C and the vacuum was approximately 27 Pa. Silicon wafers were placed around the vicinity of the furnace exit to collect the expected nanomaterials. After prolonged heating, grey layers were found on top of one wafer located inside the furnace. The layer showed no adhesion to the substrate. Characterization by using Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and Energy Dispersive X-ray Spectroscopy (EDS) revealed that this layer consisted of SiOx nanowires. Formation of Si-containing liquid drop and the subsequent growth of SiOx nanowires out of it are suggested as the growth mechanism.</p></abstract>

In an effort to synthesize doped ZnO nanowires, SiOx nanowires were obtained accidently. In the experiment, mixed powders containing chemicals such as ZnO, graphite, Ga2O3, and In2O3 were placed in the center of a tube furnace, where the temperature was set to 1200 °C and the vacuum was approximately 27 Pa. Silicon wafers were placed around the vicinity of the furnace exit to collect the expected nanomaterials. After prolonged heating, grey layers were found on top of one wafer located inside the furnace. The layer showed no adhesion to the substrate. Characterization by using Scanning Electron Microscope (SEM), Transmission Electron Microscope (TEM), and Energy Dispersive X-ray Spectroscopy (EDS) revealed that this layer consisted of SiOx nanowires. Formation of Si-containing liquid drop and the subsequent growth of SiOx nanowires out of it are suggested as the growth mechanism.

Formation of silicon oxide nanowires in nanomaterial synthesis experiments based on the usage of tube furnace

Department of Physics, Clarion University, Clarion, PA, 16214, USA

Engineering Department, Youngstown State University, Youngstown, OH, 44555, USA

Materials Science-Poland

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

In an effort to synthesize doped ZnO nanowires, SiOx nanowires were obtained accidently. In the experiment, mixed powders containing chemicals such as ZnO,...

Formation of silicon oxide nanowires in nanomaterial synthesis experiments based on the usage of tube furnace

Published Online: Aug 29, 2013

Page range: 350 - 356

DOI: https://doi.org/10.2478/s13536-013-0111-y

Keywords
silicon, oxide, nanowires

© 2013 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Formation of silicon oxide nanowires in nanomaterial synthesis experiments based on the usage of tube furnace

Published Online: Aug 29, 2013

Page range: 350 - 356

DOI: https://doi.org/10.2478/s13536-013-0111-y

Keywordssilicon, oxide, nanowires

© 2013 Wroclaw University of Technology

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

Keywords
silicon, oxide, nanowires