Cadomian protolith ages of exotic mega blocks from Bugaj and Andrychów (Western outer Carpathians, Poland) and their palaeogeographic significance

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Abstract

This study presents the first zircon U-Pb LA-MC-ICP-MS ages and whole-rock Rb/Sr and Sm/Nd data from exotic blocks (Bugaj and Andrychów) from the Western Outer Carpathians (WOC) flysch. The CL images of the zircon crystals from both samples reveal typical magmatic textures characterized by a well-defined concentric and oscillatory growth zoning. A concordia age 580.1 ± 6.0 Ma of the zircons from the Bugaj sample is considered to represent the crystallization age of this granite. The zircon crystals from the Andrychów orthogneiss yield an age of 542 ± 21 Ma, interpreted as the uppermost Proterozoic, magmatic crystallization age of the granitoid protholith. The initial (at ca. 580 Ma) 87Sr/86Sr ratios of the Bugaj granitoids (0.72997 and 0.72874) are highly radiogenic, pointing to the assimilation of an older, possibly strongly Rb enriched source to the Bugaj melt. The Nd isotope systematics (εNd580 –1.4 and 0.4) also point to a significant contribution of such a distinct mantle source. On the basis of the sequence of magmatic events obtained from U-Pb zircon ages, we suggest that exotic mega blocks deposited to the WOC basins were related to the Brunovistulicum Terrane. They belong to the group of Vendian/Cambrian granitoids representing the latest, posttectonic expression of the Cadomian cycle.

Abstract

This study presents the first zircon U-Pb LA-MC-ICP-MS ages and whole-rock Rb/Sr and Sm/Nd data from exotic blocks (Bugaj and Andrychów) from the Western Outer Carpathians (WOC) flysch. The CL images of the zircon crystals from both samples reveal typical magmatic textures characterized by a well-defined concentric and oscillatory growth zoning. A concordia age 580.1 ± 6.0 Ma of the zircons from the Bugaj sample is considered to represent the crystallization age of this granite. The zircon crystals from the Andrychów orthogneiss yield an age of 542 ± 21 Ma, interpreted as the uppermost Proterozoic, magmatic crystallization age of the granitoid protholith. The initial (at ca. 580 Ma) 87Sr/86Sr ratios of the Bugaj granitoids (0.72997 and 0.72874) are highly radiogenic, pointing to the assimilation of an older, possibly strongly Rb enriched source to the Bugaj melt. The Nd isotope systematics (εNd580 –1.4 and 0.4) also point to a significant contribution of such a distinct mantle source. On the basis of the sequence of magmatic events obtained from U-Pb zircon ages, we suggest that exotic mega blocks deposited to the WOC basins were related to the Brunovistulicum Terrane. They belong to the group of Vendian/Cambrian granitoids representing the latest, posttectonic expression of the Cadomian cycle.

1 Introduction

Despite the long period of research conducted in the Western Outer Carpathians (WOC) the genesis and tectonic evolution of their crystalline basement is still poorly recognized (e.g. Żelaźniewicz et al., 2009; Buła et al., 2015). At present the crystalline basement is hidden below thick Upper Jurassic-Neogene flysch deposits of the WOC proper (e.g. Książkiewicz, 1977; Oszczypko and Ślączka, 1985; Golonka et al., 2009). Fragments of crystalline rocks, so-called exotics (e.g. Burtanówna et al., 1937; Wieser, 1948), interpreted to be derived from uplifted ridges (cordilleras, Książkiewicz, 1953) and transported by turbidity currents and debris flows into the adjoining flysch basins, offer the opportunity to investigate the geotectonic history of these no longer existing provenance areas of the Carpathian flysch (e.g. Wieser, 1949, 1985; Książkiewicz, 1965; Oszczypko, 1975; Malik, 1978; Oszczypko et al., 2016).

A number of studies concerning the palaeogeography of the WOC have used a range of geochronological methods including K-Ar mica dating (Poprawa et al., 2004, 2005, 2006; Haber and Hałas, 2001), Th-U-total Pb monazite dating (Hanžl et al., 2000; Budzyń et al., 2008; Salata and Oszczypko, 2010; Oszczypko et al., 2016) and U-Pb zircon geochronology (Michalik et al., 2006; Poprawa et al., 2006; Budzyń et al., 2011) to constrain the timing of magmatic and metamorphic processes recorded in the exotics. The general outcome of these investigations is that numerous exclusively pre-Alpine, in parts pre-Variscan ages were determined, but no obvious correlation of stratigraphic and tectonic position and/or geography emerged. From a methodological point of view this is due to the fact that especially K-Ar mica ages are sensitive to thermal and metasomatic overprint thus obscuring any primary geochronological signal directly dating igneous or metamorphic events. This published radiometric age data set is therefore not conclusive for the unambiguous identification of protolith and metamorphic ages.

The main purpose of our study is to present and discuss zircon U-Pb ages from two exotic mega blocks (a granite from Bugaj and an orthogneiss from Andrychów), representing the alimentary crystalline basement area of the WOC flysch. Due to the size of these two exotics (> 100 m) it can safely be assumed that their loci of deposition is far more proximal to their respective shedding ridge(s) than the probably more distally derived pebbles dated in previous studies. Additionally, the latter might easily be re-sedimented making any palaeogeographic implications drawn from ages derived from such rocks severely ambiguous. The presented results provide new information to the ongoing discussion of the late Neoproterozoic palaeogeography of tectonic units which intervene between the East European Craton (Baltica) and the lithotectonic units of the Variscan orogeny (e.g. Belka et al., 2000; Nawrocki et al., 2004; Żelaźniewicz et al., 2009; Buła et al., 2015).

2 Geological background

The Western Carpathian Mountains are subdivided into the Inner Carpathians, consisting of pre-Alpine crystalline basement units covered by Late Paleozoic to mid-Cretaceous sediments (e.g. Oszczypko, 2004; Poprawa and Malata, 2006) and the Outer Carpathians, separated by the narrow, strongly tectonized Pieniny Klippen Belt (Fig. 1). The WOC are depicted as a complex nappe structure consisting of Upper Jurassic to Neogene flysch deposits, that were folded and thrusted onto the pre-Alpine European foreland during the upper Oligocene to the middle Miocene (e.g. Oszczypko, 1998, 2004; Oszczypko and Oszczypko-Clowes, 2003; Golonka et al., 2005; 2009; Oszczypko et al., 2006, Ślączka et al., 2006).

Fig. 1
Fig. 1

Simplified geological map of the Polish part of the Western Carpathians (after Żelaźniewicz el al., 2011, modified) with the location of the investigated samples (shown as yellow dots).

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

The crystalline basement constituting the pre-Alpine foreland (known only from boreholes) is divided into two basement blocks: the Upper Silesia Block (the northern part of the Brunovistulicum Terrane) to the West and the Małopolska Block to the East (Dudek, 1980; Buła, 2000; Finger et al., 2000; Żelaźniewicz et al., 2009; Buła et al., 2015). The Precambrian basement of the Upper Silesia Block is represented by a) Neoproterozoic (660–556 Ma) metamorphic and igneous rocks, b) Ediacaran anchimetamorphic flysch-type siliciclastics and c) Paleoproterozoic (2.0 Ga) metamorphic rocks with Archean (2.7 Ga) inheritance (Buła et al. 2015). The Neoproterozoic rocks of Małopolska Block are mainly represented by flysch-type series (Żelaźniewicz et al., 2009).

In the WOC several flysch basins were identified on the basis of lithostratigraphy (from south to north), i.e. the Magura, Silesian, Sub-Silesian and Skole basins (e.g. Bieda et al., 1963; Książkiewicz, 1972; Cieszkowski et al., 1985; Oszczypko, 2006). The basins were supplied with sediments from continental margins as well as from the inter-basinal elevations (ridges) separating subbasins (e.g., Książkiewicz, 1962, 1965; Unrug, 1963, 1968; Ślączka, 1986; Olszewska and Wieczorek, 2001; Poprawa et al., 2002, 2004; Golonka et al., 2008). Based on studies of palaeotransport directions it was concluded that the Brunovistulicum and/or Małopolska Terranes (external to the WOC) and the inter-basinal Silesian Ridge were the most prominent source areas of the terrigenous material (e.g. Wieser, 1949, 1985; Książkiewicz, 1965; Sikora, 1976). The Silesian Ridge developed at the boundary between Variscan and Cadomian crustal blocks of the so-called North European platform (e.g. Golonka et al., 2005; Budzyń et al., 2011). The less prominent Andrychów Ridge, recognized in the Polish WOC emerged between the Silesian and Subsilesian-Skole basins (e.g. Książkiewicz, 1960, 1977; Golonka et al., 2005) to the NNE of the Silesian Ridge. This unit is represented by several huge (> 100 m) exotic blocks, containing granitegneiss or mylonitized rocks of unknown age and Jurassic, Cretaceous and Paleogene limestones (Olszewska and Wieczorek, 2001; Ślączka et al., 2006).

3 Sampling and analytical techniques

Three samples of crystalline rocks (Bu1, Bu2 and An) from exotic mega blocks (Bugaj and Andrychów) were investigated. These blocks, located on the boundary between the Silesian and Subsilesian units, are interpreted as olistoliths of the Silesian nappe (Ślączka and Kaminski, 1998; Golonka et al., 2005; Cieszkowski et al., 2009, 2012). The samples Bu1 and Bu2 were collected in the western flow of the Cedron stream in Bugaj near Kalwaria Zebrzydowska (coordinates: 49°50’56.40”N 19°40’40.70”E; Fig. 1). The sample An, representative for the metamorphic basement rocks of the Andrychów Ridge was collected from Pańska Góra Hill, SE of Andrychów (coordinates: 49°51’10.17”N 19°21’28.95”E, Fig. 1). The two samples Bu1 and An, weighting about 25 kg each, were selected for U-Pb dating.

Whole-rock and mineral analysis

Whole-rock samples were analysed by X-ray fluorescence (XRF) for major and large ion lithophile trace Elements (LILE) and by fusion and ICP-MS for high field strength elements (HFSE) and rare earth elements (REE) in the Bureau Veritas Minerals (Canada). Preparation involved lithium borate fusion and dilute digestions for XRF and lithium borate decomposition or aqua regia digestion for ICP-MS. LOI was determined at 1000°C. REE were normalized to C1 chondrite (Sun and McDonough, 1989).

Microprobe analyses of rock-forming and accessory minerals were undertaken in the Inter-Institutional Laboratory of Microanalyses of Minerals and Synthetic Substances, Warsaw, using a Cameca SX 100 electron microprobe operating in the wavelength-dispersive spectroscopic (WDS) mode with the following conditions: 15 kV accelerating voltage, 20 nA beam current, 1–5 μm beam diameter, peak count-time of 20 s and background count-time of 10 s.

Rb-Sr and Sm-Nd whole rock isotope analysis

The Rb-Sr and Sm-Nd analytical work was performed at the Laboratory of Geochronology, Department of Lithospheric Research, University of Vienna. Rb, Sr, Sm and Nd concentrations were determined from two different sample aliquots by isotope dilution (ID) using 87Rb-84Sr and 147Sm-150Nd spikes. Rb, Sm and Nd ID samples were measured as metals from a Re (single: Rb; double: Nd and Sm) filament using a Finnigan™ MAT262 mass spectrometer, while Sr ID and isotope composition (IC) and Nd IC samples were run on a ThermoFinnigan™ Triton TI TIMS machine. Maximum total procedural blanks were < 1 ng for Sr and 50 pg for Nd and were taken as negligible. Within-run mass fractionation for Nd and Sr isotope compositions (IC) was corrected to 146Nd/144Nd = 0.7219, and 86Sr/88Sr = 0.1194, respectively. Uncertainties on the Nd and Sr isotope ratios are quoted typical as 2σm. Errors for the 87Rb/86Sr and 147Sm/144Nd ratios, respectively, are taken as ±1%, or smaller, based on iterative sample analysis and spike recalibration. During the period of investigation a 143Nd/144Nd ratio of 0.511850 ± 0.000005 (n = 5) and a 87Sr/86Sr ratio of 0.710274 ± 0.000008 (n = 5) were determined for the La Jolla (Nd) and the NBS987 (Sr) international standards, respectively. Details of techniques, accuracy and data precision of Rb-Sr and Sm-Nd isotopic measurements are given by Thöni et al. (2008).

Zircon separation, CL imaging and U-Th-Pb MC-ICP-MS dating

Zircon crystals were separated using standard techniques (crushing, hydrofracturing, washing, Wilfley table, magnetic separator and handpicking). The separation was carried out in the Institute of Geological Sciences, Polish Academy of Sciences, Cracow. Zircon grains were selected for the morphological study using scanning electron microscopy and then imaged by cathodoluminescence using a FET Philips 30 electron microscope (15 kV and 1 nA) at the Faculty of Earth Sciences, University of Silesia, Sosnowiec, Poland.

The LA-MC-ICP-MS (Laser Ablation Multi Collector ICP-MS) analytical work was performed in two sessions at the joint ICP-MS laboratory of the Department of Earth Sciences, Karl-Franzens-University Graz and the Institute of Applied Geosciences, Graz Technical University. Analytical procedures followed the methodology outlined in Klötzli et al. (2009). Zircon 206Pb/238U, 207Pb/206Pb, and 208Pb/232Th ratios and ages were determined using a 193nm Ar-F excimer laser (NewWave) coupled to a multi-collector ICP-MS (Nu Instruments Plasma II). Ablation using He as carrier gas was raster-wise according to the CL zonation pattern of the zircons. Line widths for rastering were 10–15 μm with a rastering speed of 5 μm/sec. Energy densities were 5–5.5 J/cm2 with a repetition rate of 10 Hz. The He carrier gas (0.7 l/min) was mixed with the Ar carrier gas flow prior to the ICP plasma torch. Ablation duration was 30 to 70 sec with a 30 sec gas and Hg blank measurement preceding ablation. Ablation count rates were corrected accordingly using the mean blank measurement intensities of the individual masses. Remaining counts on mass 204 were interpreted as representing 204Pb. Static mass spectrometer analysis was as follows: 238U and 232Th were measured in Faraday detectors, 208Pb, 207Pb, 206Pb, 204Pb+204Hg and 202Hg in discrete ion counter detectors. An integration time of 1 sec was used for all measurements. The ion counter - Faraday and inter-ion counter gain factors were determined before the analytical session using the reference zircon Plešovice (Sláma et al., 2008). The overall sensitivity for 206Pb on reference zircon Plešovice was c. 0.18 mV/weight-ppm 206Pb. For 238U the corresponding value was c. 0.39 mV/weight-ppm U. Isotopic ratios were calculated using the MS Excel spreadsheet LamTool U-Th-Pb version VI (Košler et al., 2008; Košler and Klötzli, unpublished). In order to avoid potential surface contamination, the signals from the first laser pass was rejected and untypical Pb-peaks, from Pb-rich inclusions, were removed in the LamTool spreadsheet. Mass and elemental bias and mass spectrometer drift of U/Pb, Th/Pb and Pb/Pb ratios, respectively, were corrected applying the “intercept method” of Sylvester and Ghaderi (1997). The calculated 206Pb/238U and 207Pb/206Pb intercept values, respectively, were corrected for mass discrimination from analyses of reference zircon Plešovice zircon (Sláma et al., 2008) measured during the analytical session using a standard bracketing method (Klötzli et al., 2009). The correction utilizes regression of standard measurements by a quadratic function. No common Pb correction was applied to the data. Final age calculations were performed with Isoplot© 3.75 (Ludwig, 2012). Reference zircon Plešovice (Sláma et al., 2008) was also used as secondary standard in order to derive an estimate of the overall uncertainties associated with the age determinations. 4 and 7 measurements where additionally made during the two analytical session, which resulted in concordia ages of 337.2 ± 3.6 Ma and 337 ± 10 Ma, respectively. These are within error identical to the accepted reference 206Pb/238U age of 337.13 ± 0.37 Ma (Sláma et al., 2008). These uncertainties where propagated in quadrature to the single dates in order to account for the overall analytical dispersion of the LA method (Klötzli et al., 2009). All errors reported for LA data are at the 2-sigma level.

4 Petrography and whole-rock geochemistry

Bugaj granite mega block

The samples collected from the Bugaj mega block are coarse-grained granite (Bu1, Fig. 2a, Fig. 3) to granodiorite (Bu2, Fig. 3), lacking any visible orientation, locally porphyritic. They are composed of pinkish K-feldspars (Or91-93Ab5-6Cn1-2), weakly zoned oligoclase (An18-25), biotite showing a brown-yellow pleochroism (Ti = 0.38– 0.42 a.p.f.u.; #fm = 0.65–0.66), locally replaced by chlorite and associated with secondary rutile. Accessory minerals are (Ca, F)-apatite and zircon. Sporadically rounded monzonitic enclaves up to 5–10 cm in size can be found, showing a sharp contact with the surrounding host rock. The enclaves are composed of fine-grained biotite (Ti = 0.30–0.38 a.p.f.u.), oligoclase (An20-26), and quartz. Accessory (Ca, F)-apatite is also observed (BuC, Fig. 3).

Fig. 2
Fig. 2

Field photo (a) of the Bugaj granitoid (sample Bu1) and field photo (b) of the Andrychów orthogneiss (sample An).

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Fig. 3
Fig. 3

Classification position of the Bugaj granitoids in: (a) alkali (K2O + Na2O) versus SiO2 (TAS) classification diagram (Middlemost, 1985); (b) Primitive mantle-normalized (Sun and McDonough, 1989) multielement “spider” diagrams; (c) classification position of the Bugaj granitoids in Multicationic R1–R2 diagram (De La Roche et al.,1980), with fields numbered according to Batchelor and Bowden (1985); 1 – mantle fractionates, 2 – pre-plate collision suites, 3 – post-collision suites, 4 – late orogenic magmas, 5 – anorogenic suites, 6 – syncollisional (anatectic) suites. R1 = 4Si − 11(Na + K) − 2(Fe + Ti); R2 = 6Ca + 2 Mg + Al.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Studied rocks are peraluminous (ASI = 1.16–1.23) with silica contents around 60–71 wt.%, K2O ≥ Na2O and Rb/Sr ratios = 1.1–1.4 (Table 1). The rocks belong to the high K-calc-alkaline series and are intermediate between the ferroan and magnesian families of the Frost and Frost (2008) geochemical classification. Chondrite-normalized (Sun and McDonough, 1989) REE patterns show low LREE enrichment (CeN/YbN = 3.18–6.34) and a strong negative Eu anomaly (Eu/Eu* = 0.38–0.57; Table 1; Fig. 3b). Magma crystallization temperatures calculated on the basis of the Zr-saturation geothermometer of Watson and Harrison (1983) are in the range of 800–850°C

(Table 1). The primitive-mantle-normalized multielement diagram points to an arc-setting of the magma, with typical Nb and Ta negative anomalies, whereas the Batchelor and Bowden (1985) classification suggests a post-collisional to late-orogenic magmatic suite (Fig. 3b, 3c). Granodiorite-granite rocks show relatively high

Table 1

Chemical composition and selected petrological indicators of Bugaj granitoid rocks.

Sample NoBu1Bu2BuC
SiO271.5667.5860.03
TiO20.380.70.98
Al2O314.1314.8916.63
Fe2O3T3.045.318.32
MnO0.060.090.14
MgO0.771.342.46
CaO0.921.51.89
Na2O3.363.833.33
K2O4.793.364.86
P2O50.110.220.18
LOI0.711.130.9
Total99.8399.9599.72
Sr121.2128152.3
Ba578562793
Rb135.6146.9219.3
Cs8.310.313.1
Th1111.71.3
U2.61.410.1
Ga1620.420.5
Cr82109.5116.3
Ni111427.9
V4375135
Zr150.9283.6226.8
Hf4.97.66.2
Y42.937.927
Nb9.815.416.1
Ta0.81.10.9
La24.630.327.9
Ce52.662.461.9
Pr6.357.567.06
Nd24.730.627.3
Sm5.966.635.64
Eu0.750.871.01
Gd6.046.95.45
Tb0.990.990.89
Dy6.966.974.9
Ho1.491.30.95
Er4.323.623.1
Tm0.690.560.41
Yb4.563.672.69
Lu0.640.50.42
ASI1.171.231.21
#mg0.560.70.31
Rb/Sr1.121.151.44
ΣREE140.65162.87149.62
Eu/Eu*0.80.390.56
CeN/YbN3.184.686.34
ThN/UN1.042.060.03
TZr [°C]798850818
ExplanationsLoD – limits of detection; LOI – loss of ignition; Eu/Eu* = Eu/Sm·Gd; ASI = Al2O3/(CaO + Na2O + K2O − 3.33 P2O5) (in molecular values); TZr = temperature calculated according to Watson and Harrison (1983) procedure.

ThN/UN ratios (2.06 and 1.05 respectively), whereas the monzonitic enclave shows a strong positive U anomaly and a ThN/UN ratio of 0.03, suggesting a highly oxidised source (possibly mantle-type?) of the monzonitic magma (Fig. 3b; Table 1).

The whole-rock isotope geochemistry data of two Bugaj mega block samples are presented in Table 2 Both samples (Bu1, Bu2) show nearly identical 87Rb/86Sr ratios (3.154 ± 0.032 and 3.236 ± 0.032) as well as 87Sr/86Sr ratios (0.756053 ± 0.000004 and 0.755499 ± 0.000004). The initial 87Sr/86Sr(580 Ma) ratios are 0.72997 and 0.72874.

Table 2

Rb-Sr and Sm-Nd whole rock isotope analysis of Bugaj granitoid rocks.

Isotope data87Rb/86Sr±2sm87Sr/86Sr±2sm147Sm/144Nd±2sm143Nd/144Nd±2smSr(580 Ma)Nd(580 Ma)Nd(CHUR)
Bugaj13.1540.0320.7560530.0000040.15210.00150.5123970.0000040.7299660.511819–1.4
Bugaj23.2360.0320.7554990.0000040.13660.00140.5124280.0000050.7287390.5119090.4

Contrary to the above the Sm-Nd isotope systematics of the two Bugaj mega block samples are dissimilar: 147Sm/144Nd ratios are 0.1521 ± 0.0015 (Bu1) and 0.1366 ± 0.0014 (Bu2). The 143Nd/144Nd ratios are 0.512397 ± 0.000004 and 0.512428 ± 0.000005, respectively. The resulting εNd580 are –1.4 and 0.4.

Andrychów orthogneiss mega block

The sample (An) is a medium-grained augen gneiss (Fig. 2b), consisting of quartz, K-feldspar, plagioclase (An10-18) and biotite. The foliation is defined by biotite, quartz ribbons and elongate feldspars. Accessory minerals are apatite and zircon. Due to the penetrative low-temperature and structural overprinting of the Andrychów mega block rocks, no detailed micro-chemical analyses, whole rock chemistry as well as Rb-Sr and Sm-Nd isotope whole rock geochemistry were obtained.

5 Zircon characteristics and U-Pb ages

Bugaj mega block

The zircons are colourless or slightly pink, euhedral, normal to very long-prismatic, even to acicular (aspect ratios 1:1 to 1:10). Grain sizes vary in length from ca. 50 to 350 μm (Fig. 4). A small percentage of zircon grains show an unusual habit contrasting markedly with the prismatic and acicular crystals (Fig. 4, p6Bu81). This habit is tabular, strongly flattened on the [110] crystal face (elongation ratio < 1). The typology falls into the S4 subtype group of Pupin (1980).

Fig. 4
Fig. 4

Secondary electron (SE) images of selected zircon crystals from granite sample Bu1. See text for description.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

The cathodoluminescence (CL) images reveal a complexity of the internal structure. A significant number of crystals shows igneous oscillatory growth zoning, with growth bands varying between fine and broad within individual grains (Fig. 5). Luminescence is variable, but mostly moderate. Some grains display a blurred, light grey zonation, present in the centre of the zircon crystals (Fig. 5, p3Bu01). A small number of inherited cores were observed in normal-prismatic crystals (Fig. 5).

Fig. 5
Fig. 5

Compiled cathodoluminescence (CL) images showing the range of textures observed in zircon crystals from granite sample Bu1. See text for details. The white rectangles show the approximate location of laser ablation trenches (confirmed by re-inspecting grains under CL after the LA analysis) and are not to scale. The numbers refer to the analytical data presented in Table 3.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Table 3

LA-MC-ICP-MS U–Pb zircon data from exotic mega blocks (samples An and Bu1).

SampleBlank corrected intensitiesConcentrationsAtomic ratiosAges
Crystal204Pb206Pb207Pb208Pb232Th238UPbThUTh/U206Pb 204Pb2RSE207Pb 235U2RSE206Pb 238U2RSE207Pb Rho 206Pb2RSE208Pb 206Pb2RSE208Pb 232Th2RSE238U 206Pb2RSE207Pb 206Pb2RSE206/238 age2SD206/207 age2SD
(V) ×10-6(V) ×10-4(V) ×10-5×(10V) -5×(10V) -3(V) ×10-2(wppm)(%)(%)(%)(%)(%)(%)(%)(%)(Ma)
Andrychów An
p3An_026.1039.023.051.011.06.3010.124.4139.90.1790880.67163.90.07953.80.48 0.06061.30.43164.90.03166.912.5753.80.06061.34931962429
p3An_03/17.0068.041.097.028.010.017.764.8140.60.461037200.80446.30.08948.30.65 0.06424.30.499416.00.022813.111.1898.30.06424.35524675092
p3An_03/215.065.047.092.018.013.017.241.5141.10.29810270.669810.30.072517.40.85 0.068116.10.414511.50.035722.513.79917.40.068116.145178871334
p3An_04/14.2042.023.037.09.606.2010.421.9139.90.16124180.704311.80.087310.80.46 0.05871.30.244011.80.025310.611.44810.80.05871.35405855429
p3An_04/24.9035.020.041.011.04.909.125.3139.70.181130100.717812.00.08859.60.40 0.05912.50.34776.10.022410.311.2959.60.05912.55475357254
p3An_06/14.4012014022014.03.7033.331.8139.50.233187147.210612.50.395613.20.53 0.13191.30.57784.20.087025.52.52813.20.13191.32149284212323
p3An_06/25.0019020098.07.909.2047.118.1140.40.13ndnd4.24987.30.26508.70.59 0.11381.10.166923.50.084910.13.7748.70.11381.11515132186120
p3An_074.7064.038.080.025.010.016.558.1140.50.411767160.71389.90.080014.20.71 0.06463.70.35298.50.021914.512.50014.20.06463.74967076179
p3An_085.0015014017017.08.0039.939.3140.20.283863153.034315.20.231715.50.51 0.09470.50.33185.80.069610.84.31615.50.09470.5134320815219
p3An_096.6070.043.012031.010.018.870.9140.50.501540150.84389.60.093311.50.60 0.06443.70.49837.20.026710.510.71711.50.06443.75756675379
p3An_105.8055.032.093.028.07.2014.763.3140.10.45125920.80635.70.09505.60.49 0.06130.90.44592.90.02248.310.5235.60.06130.95853364920
p3An_116.9024.017.033.08.53.506.319.4139.50.14580190.932510.90.09699.30.43 0.06908.60.337112.20.026115.110.3179.30.06908.659655899177
p3An_12/14.6047.027.010.02.26.9011.05.1140.00.04ndnd0.69938.50.08509.10.53 0.05950.70.05688.10.03017.211.7649.10.05950.75264858715
p3An_12/24.9019.012.016.05.52.404.812.5139.30.09473111.017417.20.113415.90.46 0.06423.80.298940.00.020418.48.82115.90.06423.869211075080
p3An_1325.052.067.011019.013.015.143.7141.10.31193400.969111.90.050722.80.96 0.148117.20.623526.80.078039.619.74122.80.148117.2319732324295
Bugaj Bu1
p2Bu_0114.044.037.063.012.05.8011.827.5139.80.20341140.87055.00.09474.00.40 0.06243.70.26057.20.02097.410.5604.00.06243.75832368879
p2Bu_05nd44.028.085.012.04.5012.027.2139.60.19ndnd0.87376.30.10716.60.52 0.05920.90.593620.80.02638.79.3416.60.05920.96564357319
p2Bu_086.8058.038.081.011.06.6015.326.3140.00.191018110.73786.40.08967.10.55 0.05971.10.35248.20.02176.611.1577.10.05971.15533959225
p2Bu_10/150.085.093.018019016.024.6435.3141.53.089311870.794238.60.1102177.82.31 0.028713560.065036670.0207217.69.073177.80.028713566741199--
p2Bu_10/225.018012027038.020.047.887.8142.30.6294660.79128.60.09289.00.52 0.06112.90.302910.60.02217.910.7769.00.06112.95725264362
p2Bu_1917.089.057.076.09.7010.022.422.1140.60.16ndnd0.76383.20.09673.10.49 0.05750.40.304442.10.02445.910.3393.10.05750.4595185109
p2Bu_2314.011013027011.04.3033.526.1139.60.1999214.67045.00.31214.50.45 0.10841.30.50184.70.07516.13.2044.50.10841.3175178177325
p2Bu_307.8088.056.017022.010.024.050.8140.60.36ndnd0.78069.30.09787.60.41 0.05781.70.364933.30.023714.510.2297.60.05781.76014652437
2Bu_329.9054.035.050.05.805.9013.713.3139.90.0980130.74875.20.09315.60.54 0.05840.70.211322.70.02695.110.7425.60.05840.75743254615
p2Bu_35/18.6059.038.053.06.106.9014.814.1140.00.1072380.72955.20.08777.30.70 0.05982.10.268425.80.025216.011.4057.30.05982.15424059745
p2Bu_35/27.8084.056.039.04.108.9020.49.5140.40.07863740.811924.60.096034.00.69 0.06066.90.1682122.60.035636.310.42034.00.06066.9591201624149
p3Bu_01/111.061.051.069.055.012.015.8125.9140.90.89546300.77738.60.06924.30.25 0.08399.00.417120.20.012821.314.4604.30.08399.0431191290176
p3Bu_01/24.6015.011.017.011.02.103.825.3139.20.18ndnd0.873017.30.094611.90.35 0.064619.50.337154.80.019824.310.56911.90.064619.558369762412
p3Bu_01/317.048.042.012083.08.3014.0189.3140.31.35453220.86956.40.08009.10.71 0.081410.40.959919.50.021815.012.5069.10.081410.4496451232204
p3Bu_03/1nd1.801.101.200.7400.2500.41.7138.90.01ndnd0.932536.60.114539.40.54 0.05996.20.229015.00.0153106.68.73639.40.05996.2699276599135
p3Bu_03/24.200.7800.510.570.3900.1100.20.9138.90.0140110.925814.20.110413.40.47 0.06094.30.23336.90.019616.79.05413.40.06094.36759063692
p3Bu_044.000.9800.670.500.3500.1500.20.8138.90.01ndnd0.844221.70.093023.30.54 0.06469.00.172620.30.014070.510.74923.30.06469.0573133761189
p3Bu_09/142.033.052.012076.07.3010.8175.0140.11.25199252.1793196.90.1178133.30.34 0.102196.80.7533129.50.0158695.38.488133.30.102196.871895716631791
p3Bu_09/25.8035.024.075.029.05.509.766.8139.80.4872040.81874.00.09262.40.29 0.06453.60.919617.50.02794.410.7992.40.06453.65711375876
p3Bu_10nd16.010.030.012.02.504.426.7139.30.19ndnd0.78261.90.09561.70.44 0.05920.60.64393.70.02842.210.4591.70.05920.65891057613
p3Bu_125.4032.020.031.012.04.908.126.9139.70.1956760.759311.70.093610.20.44 0.05883.20.4832241.30.028719.410.67910.20.05883.25775955969
p3Bu_13/14.6024.015.023.08.103.606.018.6139.50.13ndnd0.77623.90.09434.90.63 0.05961.90.501675.80.029521.610.6034.90.05961.95812858941
p3Bu_13/26.8015.09.908.106.402.303.614.7139.30.11346610.844339.70.090821.50.27 0.067027.50.2070122.80.0159110.511.01421.50.067027.5560120838573
p3Bu_144.0016.09.8015.05.902.404.013.4139.30.10119150.74774.00.08924.60.58 0.06070.90.590520.30.02885.211.2164.60.06070.95512563020
p3Bu_155.302.101.603.201.700.3200.64.0138.90.0352120.967014.20.090513.80.49 0.07627.90.517612.70.019617.111.04513.80.07627.9559771099158
2RSE 2-sigma relative standard error (in %), Rho the error correlation between the 206/238 and 207/235 ratios.

Crystal domains targeted for dating are characterized by the presence of a well-developed fine-scale oscillatory growth zonation (Fig. 5). 25 dates on 19 crystals were gained (Table 3, Fig. 5). Individual 206Pb/238U dates range from 1751 ± 78 Ma to 431 ± 19 Ma, whereas 207Pb/206Pb dates range from 1773 ± 25 Ma to 510 ± 9 Ma, respectively. No systematic difference between the two populations could be detected. Thus the final age calculation took into account all analysed crystals of the Bugaj1 sample. One analysis (Bugaj1_p2bu_023A) is concordant at an age of ca. 1760 Ma (Fig. 6a). 14 dates form a sub-concordant (discordance < 5%) cluster with a lower intercept date of 580.1 ± 6.0 Ma (Fig. 6b, model 1 solution, anchored at 207Pb/206Pb = 0.85 ± 0.05, MSWD = 1.8, Probability of fit = 0.031). These crystals show a mean Th/U of 0.16 ± 0.07. Three sub-concordant analyses (discordance < 5%), characterized by comparably high Th/U (0.30 ± 0.04), form a cluster with a lower intercept date of 662 ± 37 Ma (not shown, model 1 solution, anchored at 207Pb/206Pb = 0.85 ± 0.05, MSWD = 0.12, Probability of fit = 0.89). This lower intercept date is statistically distinguishable from the former one, also based on the disparate Th/U ratios of the two clusters. The remaining 7 analyses are highly discordant with high Th/U ratios (0.72 ± 0.35), again statistically distinguishable from the former two clusters.

Fig. 6
Fig. 6

Tera-Wasserburg diagrams presenting the U/Pb age of the zircons from granite sample Bu1: a) all data points; b) concordant to sub-concordant data points. The inherited xenocryst (p2Bu_23) and the three data points showing recent lead loss (p3Bu_01/1, p3Bu_01/1, p3Bu_09/1) are not shown.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Andrychów mega block

Zircon grains are euhedral, up to 300 μm long, with aspect ratios from 1:1 to 1:3 (Fig. 7). They are clear, yellow and greenish yellow in colour.

In CL images a variably developed oscillatory growth zoning is the prominent feature of all analysed grains, as shown by moderate to weak luminescence. Some crystals display core-rim structures. The cores are characterized by oscillatory growth zoning with high/moderate CL intensity (Fig. 8).

Fig. 7
Fig. 7

Secondary electron (SE) images of selected zircon crystals from orthogneiss sample An. See text for description.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Fig. 8
Fig. 8

Compiled cathodoluminescence (CL) images showing the range of textures observed in zircon crystals from orthogneiss sample An. See text for details. The white rectangles show the approximate location of laser ablation trenches (confirmed by re-inspecting grains under CL after the LA analysis) and are not to scale. The numbers refer to the analytical data presented in Table 3.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

Crystal domains targeted for dating are characterized by the presence of a well-developed fine-scale oscillatory growth zonation (Fig. 8). 15 dates on 10 crystals were gained (Table 3, Fig. 8). Individual 206Pb/238U dates range from 2149 ± 284 Ma to 319 ± 73 Ma, whereas 207Pb/206Pb dates range from 2324 ± 295 Ma to 554 ± 29 Ma, respectively. One analysis (Andrychów_p3an_06A) is concordant at an age of 2123 ± 23 Ma (Fig. 9a). 7 dates form a sub-concordant (discordance < 5%) cluster with a mean Th/U of 0.23 ± 0.11. Two lower intercept dates can be calculated: i) 549 ± 29 Ma with an upper intercept at 2432 ± 1500 Ma (not shown, model 1 solution, MSWD = 0.99, Probability of fit = 0.42); ii) 542 ± 21 Ma with the upper intercept fixed at 2123 ± 23 Ma of analysis Andrychów_p3an_06A (Fig. 9b, model 1 solution, MSWD = 0.86, Probability of fit = 0.53).

Fig. 9
Fig. 9

Tera-Wasserburg diagrams for isotopic ratio for zircon crystals from orthogneiss sample An: a) all data points; b) concordant to sub-concordant data points defining a discordia line with a lower intercept of 542 ± 21 Ma (forced through data point p3An_06/1). The inherited xenocrysts (p3An_06/1, p3An_06/2) and the two data points showing recent lead loss (p3An_08, p3An_13) are not shown.

Citation: Geochronometria 46, 1; 10.1515/geochr-2015-0102

The calculated upper intercept value of 2432 ± 1500 Ma of i) is well within uncertainty with the concordant age value of 2123 ± 23 Ma used for the calculation in ii). Also the two lower intercept ages are identical within their uncertainty limits.

The remaining analyses either are strongly discordant (discordance > 10%) or sub-concordant (discordance < 5%) at 207Pb/206Pb ages between 2324 ± 295 Ma and 624 ± 29 Ma. The Th/U ratios of these analyses are identical to the former one (0.18 ± 0.06).

6 Discussion

Exotics represent one of the most important sources of information about Carpathian alimentary areas, indirectly indicating their geotectonic history. For both exotic mega blocks (sample Bugaj and sample Andrychów) igneous formation ages were derived from the zircon U-Pb data.

The Cadomian age (580.1 ± 6.0 Ma) from sample Bu1 is interpreted as magmatic crystallization age of the Bugaj granitoids. A fine-scale oscillatory zonation in the CL images as well as Th/U ratio of 0.16 ± 0.07 point to igneous crystal growth (Corfu et al., 2003). Three analyses (Th/U ratios 0.30 ± 0.04), forming a cluster with a lower intercept age of 662 ± 37 Ma are interpreted to reflect a major contribution from a single inheritance source to the ca. 580 Ma igneous event. The singular 207Pb/206Pb age of 1773 ± 25 Ma (p2Bu_23) represents a xenocryst.

The Sr and Nd whole-rock isotope data are controversial. The initial (at ca. 580 Ma) 87Sr/86Sr ratios of the Bugaj granitoids (0.72997 and 0.72874) are highly radiogenic, pointing to the assimilation of an older, possibly strongly Rb enriched source to the Bugaj melt. On the other hand, the Nd isotope systematics (εNd580 –1.4 and 0.4) rather point to a significant contribution of a distinct mantle source to the Bugaj melt. These geochemical data thus allow to recognize a hybrid geochemical character of the investigated rocks and/or decoupling of the Rb-Sr and Sm-Nd isotopic systems during post-magmatic alteration also supported by the presence of mafic enclaves. Such a hybrid character is also reflected in the high K-calcalkaline series affinity with the intermediate association of the ferroan and magnesian families (Frost and Frost, 2008). Also the relatively high ThN/UN ratios (2.06 and 1.05) are remarkably well reflected in the high Th/U ratios of some zircon domains (0.72 ± 0.35). It is not clear, whether this hybridisation is a primary one, i.e. occurring during protolith formation or a secondary one.

The biotite K-Ar age of 485 ± 10 Ma (Haber and Hałas, 2001) indicates either slow cooling to ca. 300°C after the 580 Ma magmatic event or a Lower Ordovician thermal and possibly fluid-related overprint, which might have caused the resetting of the Rb-Sr system which resulted in highly radiogenic 87Sr/86Sr ratios. It has to be noticed however, that such an event is not detected in the U-Pb zircon data. This fact is in favour of the slow cooling model.

In the Andrychów sample, the lower intercept age of 542 ± 21 Ma, obtained from zircon domains exhibiting a fine-scale oscillatory growth zonation in the CL images, is interpreted as the uppermost Proterozoic to Cambrian magmatic crystallization age of the granitic precursor of the orthogneiss. The concordant age at 2123 ± 23 Ma represents Palaeoproterozoic inheritance. There is no evidence for a Variscan (Devonian-Carboniferous) or Alpine (Neogene) metamorphic overprint, neither from the zircon U-Pb age systematics nor from the zircon mineral chemistry, i.e. the Th/U ratios (samples Bu1 and An), and the whole-rock isotope geochemistry (sample Bu1). Lack of any Variscan overprint suggests no similarities of the analysed exotic mega blocks to the crystalline basement of the Inner Western Carpathians, showing the Variscan consolidation, e.g. from granitoids of the Tatra Massif (e.g. Burda and Klötzli, 2011; Burda et al., 2013).

The U-Pb zircon ages presented in this study are consistent with published results (monazite Th-U-total Pb dating, K-Ar dating of muscovite and biotite), reported from clastic material supplying Silesian basin from the Brunovistulicum and/or Małopolska Terranes as northern source areas (Poprawa et al., 2004, 2005, 2006; Budzyń et al., 2008, 2011).

The sequence of events obtained from U-Pb zircon ages from Bugaj and Andrychów exotic mega blocks shows similarities to magmatic-metamorphic events identified in the Brunovistulicum Terrane. These events include: a) terrane collision with deformation, metamorphism and plutonism at ca. 650–620 Ma; b) arc-type granitoid intrusions at ca. 590–580 Ma and c) late bimodal magmatism and strike-slip deformation at ca. 560–550 Ma. No evidence for Variscan magmatism and/or metamorphism has emerged (e.g. Finger et al., 2000; Żelaźniewicz et al., 2009 and references therein). Also the εNd580 (–1.4 and 0.4) obtained for the Bugaj granitoid is similar to the Neoproterozoic igneous rocks from the Brunovistulicum Terrane having εNd580 values ranging from –1 to +3 (Finger et al., 2000).

Our investigations thus support the connection of the exotic mega blocks with the Avalonian-Cadomian orogenic belt during the Neoproterozoic (Żelaźniewicz et al., 2009).

7 Conclusions

  1. For both exotic mega blocks (Bugaj and Andrychów) igneous formation ages could be derived from the zircon U-Pb data. These are 542 ± 21 Ma for the orthogneiss from Andrychów and 580.1 ± 6.0 Ma for the granitoid from Bugaj.
  2. The U-Pb zircon ages, derived from > 100 m sized exotic mega blocks, directly reflect the presence of substantial amounts of a proximal ‘Cadomian’ aged crust proper in the vicinity of the WOC basement. This is a marked difference to earlier published data, which are derived from cm-dm sized pebbles only. As these can easily be derived from re-sedimented sources the ages do not necessarily reflect direct derivation from a ‘Cadomian’ basement, inasmuch as transport distances are not known.
  3. Exotic mega blocks deposited to the WOC basins were related to the Brunovistulicum Terrane. They belong to the group of Vendian/Early Cambrian granitoids, representing the latest, post-tectonic expression of the Cadomian cycle.
Acknowledgements

We are grateful to Ewa Teper (University of Silesia in Katowice) for help with CL investigations. Monika Horschinegg (University of Vienna) is thanked for help with the Rb-Sr and Sm-Nd isotope determinations. Christoph Hauzenberger (Karl-Franzens University Graz) and Dorothee Hippler (Technical University Graz) kindly provided access to their joint LA-MC-ICP-MS facility. Financial means provided by the DS found of the University of Silesia in Katowice to JB and BWŚ, by the Austrian Science Fund FWF to UK (FWF M-1371-N19) and by the Polish National Science Centre (NCN) UMO-2016/23/B/ST10/01896 to AG are also acknowledged. Reviews by Hans-Joachim Massonne and the anomynous referee are highly appreciated.

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  • Oszczypko N Oszczypko-Clowes M and Salata D 2006. Egzotyki strefy krynickiej (płaszczowina magurska) magurska ich znaczenie paleogeograficzne (Exotic rocks of the Krynica Zone (Magura nappe) and their palaeogeographic significance). Geologia 32(1): 21–45 (in Polish).

  • Oszczypko N Salata D Konečny P 2016. Age and provenance of mica-schist pebbles from the Eocene conglomerates of the Tylicz and Krynica Zone (Magura Nappe Outer Flysch Carpathians). Geologia Carpathica 67: 260–274.

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    • Export Citation
  • Poprawa P Malata T and Oszczypko N 2002. Ewolucja tektoniczna basenów sedymentacyjnych polskiej części Karpat zewnętrznych w świetle analizy subsydencji (Tectonic evolution of the Polish part of Outer Carpathian's sedimentary basins - constraints from subsidence analysis). Przegląd Geologiczny 50: 1092–1108 (in Polish).

  • Poprawa P Malata T Pécskay Z Banaś M Skulich J Paszkowski M and Kusiak MA 2004. Geochronology of crystalline basement of the Western Outer Carpathians' sediment source areas. Polskie Towarzystwo Mineralogiczne — Prace Specjalne 24: 329–332.

  • Poprawa P Kusiak MA Malata T Paszkowski M Pécskay Z and Skulich J 2005. Th–U–Pb chemical dating of monazite and K/Ar dating of mica combined: preliminary study of “exotic” crystalline clasts from the Western Outer Carpathian flysch (Poland). Polskie Towarzystwo Mineralogiczne — Prace Specjalne 25: 345–351.

  • Poprawa P Malata T Pécskay Z Kusiak MA Banaś M and Paszkowski M 2006. Geochronology of the crystalline basement of the Western Outer Carpathians' source areas — constraints from the K/Ar dating of mica and Th–U–Pb chemical dating of monazite from the crystalline ‘exotic’ pebbles. Geolines 20: 110–112.

  • Poprawa P and Malata T 2006. Model of Late Jurassic to Early Miocene tectonic evolution of the Western Outer Carpathians. Przegląd Geologiczny 54: 1066–1080 (in Polish).

  • Pupin JP 1980. Zircon and Granite Petrology. Contributions to Mineralogy and Petrology 73: 207–220 DOI 10.1007/BF00381441.

    • Crossref
    • Export Citation
  • Salata D and Oszczypko N 2010. Preliminary results of provenance analyses of exotic magmatic and metamorphic rock pebbles from the Eocene flysch deposits of the Magura Nappe (Krynica facies zone Polish Outer Carpathians). In: Christofidis G Kantiranis N Kostopoulos DN and Chatzipetros AA eds. Proceedings of the XIX CBGA Congress Thessaloniki Greece Scientific Annals School of Geology Aristotle University of Thessaloniki special volume 100: 241–249.

  • Sikora WJ 1976. Kordyliery Karpat Zachodnich w świetle tektoniki płyt litosfery (Cordilleres of the Western Carpathians in the light of the plate tectonics theory). Przegląd Geologiczny 6: 336–349 (in Polish).

  • Sláma J Košler J Condon DJ Crowley JL Gerdes A Hanchar JM. Horstwood MSW Morris GA Nasdala L Norberg N Schaltegger U Schoene B Tubrett MN and Whitehouse MJ 2008. Plešovice zircon – a new natural reference material for U-Pb and Hf isotopic microanalysis. Chemical Geology 249: 1–35 DOI 10.1016/j.chemgeo.2007.11.005.

    • Crossref
    • Export Citation
  • Ślączka A 1986. Europejskie spotkania sedymentologów (European sedimentologists' meetings). Przegląd Geologiczny 34(4): 231.

  • Ślączka A and Kaminski MA 1998. A Guidebook to Excursions in the Polish Flysch Carpathians. Grzybowski Foundation Special Publication 6: 171 pp.

  • Ślączka A Krugłov S Golonka J Oszczypko N and Popadyuk I 2006. Geology and Hydrocarbon Resources of the Outer Carpathians Poland Slovakia and Ukraine: General Geology. In: Golonka J and Picha FJ eds. The Carpathians and their foreland: Geology and hydrocarbon resources. AAPG Memoir 84: 221–259.

  • Sun SS and McDonough WF 1989. Chemical and isotopical systematics of oceanic basalts: implications for mantle composition and processes. Magmatism in the Oceanic Basins. Geological Society of London Special Pubplications 42: 313–345.

    • Crossref
    • Export Citation
  • Sylvester PJ and Ghaderi M 1997. Trace element analysis of scheelite by excimer laser ablation-inductively coupled plasma-mass spectrometry (ELA-ICP-MS) using a synthetic silicate glass standard. Chemical Geology 141: 49–65 DOI 10.1016/S0009-2541(97)00057-0.

    • Crossref
    • Export Citation
  • Thöni M Miller C Zanetti A Habler G and Goessler W 2008. Sm–Nd isotope systematics of high-REE accessory minerals and major phases: ID-TIMS LA-ICPMS and EPMA data constrain multiple Permian-Triassic pegmatite emplacement in the Koralpe Eastern Alps. Chemical Geology 254: 216–237 DOI 10.1016/j.chemgeo.2008.03.008.

    • Crossref
    • Export Citation
  • Unrug R 1963. Istebna beds - a fluxoturbidity formation in the Carpathian Flysch. Rocznik Polskiego Towarzystwa Geologicznego 33: 49–92.

  • Unrug R 1968. Kordyliera śląska jako obszar źródłowy materiału klastycznego piaskowców fliszowych Beskidu Śląskiego i Beskidu Wysokiego (Polskie Karpaty zachodnie) (The Silesian cordillera as the source of clastic material of the Flysch sandstones of the Beskid Śląski and Beskid Wysoki ranges (Polish Western Carpathians). Rocznik Polskiego Towarzystwa Geologicznego 38: 81– 164.

  • Watson TM and Harrison EB 1983. Zircon saturation revisited: temperature and composition effects in a variety of crustal magma types. Earth and Planetary Science Letters 64: 295–304 DOI 10.1016/0012-821X(83)90211-X.

    • Crossref
    • Export Citation
  • Wieser T 1948. Crystalline exotic blocks in the Silesian Cretaceous of the Wadowice area (Pl. I-II). Annales Societatis Geologorum Poloniae 18: 36–150 (in Polish).

  • Wieser T 1949. Egzotyki krystaliczne w kredzie śląskiej okolic Wadowic (Crystalline exotic blocks in the Silesian Cretaceous of the Wadowice area). Rocznik Polskiego Towarzystwa Geologicznego 18: 36–105 (in Polish).

  • Wieser T 1985. Some remarks on the sedimentation composition and provenance of exotic bearing conglomerates in the western Polish Carpathians Flysch formations. 13th Congress Carpatho-Balkan Geological Association Guide 1. Geological Institute Kraków: 57–68.

  • Żelaźniewicz A Buła Z Fanning M Seghedi A and Żaba J 2009. More evidence on Neoproterozoic terranes in Southern Poland and south eastern Romania. Geological Quarterly 58(1): 93–124.

  • Żelaźniewicz A Aleksandrowski P Buła Z Karnkowski PH Konon A Oszczypko N Ślączka A Żaba J and Żytko K 2011. Regionalizacja tektoniczna Polski (Tectonic regionalization of Poland). Komitet Nauk Geologicznych PAN Wrocław: 59 pp (in Polish).

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  • Budzyń B Dunkley DJ Kusiak MA Poprawa P Malata T Skiba M and Paszkowski M 2011. SHRIMP U-Pb zircon chronology of the Polish Western Outer Carpathians source areas. Annales Societatis Geologorum Poloniae 81: 161–171.

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  • Książkiewicz M (ed.) 1962. Geological Atlas of Poland. Stratigraphic and facial problems Fasc. 13 — Cretaceous and Tertiary in the Polish External Carpathians 1:600 000. Państwowy Instytut Geologiczny Warszawa.

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  • Oszczypko N and Ślączka A 1985. An attempt to palinspastic reconstruction of Neogene basins of the Carpathian Foredeep. Annales Societatis Geologorum Poloniae 55(1–2): 55–75.

  • Oszczypko N and Oszczypko-Clowes M 2003. The Aquitanian marine deposits in the basement of the Polish Western Carpathians and its paleogeographical and paleotectonic implications. Acta Geologica Polonica 53(2): 1–22.

  • Oszczypko N Oszczypko-Clowes M and Salata D 2006. Egzotyki strefy krynickiej (płaszczowina magurska) magurska ich znaczenie paleogeograficzne (Exotic rocks of the Krynica Zone (Magura nappe) and their palaeogeographic significance). Geologia 32(1): 21–45 (in Polish).

  • Oszczypko N Salata D Konečny P 2016. Age and provenance of mica-schist pebbles from the Eocene conglomerates of the Tylicz and Krynica Zone (Magura Nappe Outer Flysch Carpathians). Geologia Carpathica 67: 260–274.

    • Crossref
    • Export Citation
  • Poprawa P Malata T and Oszczypko N 2002. Ewolucja tektoniczna basenów sedymentacyjnych polskiej części Karpat zewnętrznych w świetle analizy subsydencji (Tectonic evolution of the Polish part of Outer Carpathian's sedimentary basins - constraints from subsidence analysis). Przegląd Geologiczny 50: 1092–1108 (in Polish).

  • Poprawa P Malata T Pécskay Z Banaś M Skulich J Paszkowski M and Kusiak MA 2004. Geochronology of crystalline basement of the Western Outer Carpathians' sediment source areas. Polskie Towarzystwo Mineralogiczne — Prace Specjalne 24: 329–332.

  • Poprawa P Kusiak MA Malata T Paszkowski M Pécskay Z and Skulich J 2005. Th–U–Pb chemical dating of monazite and K/Ar dating of mica combined: preliminary study of “exotic” crystalline clasts from the Western Outer Carpathian flysch (Poland). Polskie Towarzystwo Mineralogiczne — Prace Specjalne 25: 345–351.

  • Poprawa P Malata T Pécskay Z Kusiak MA Banaś M and Paszkowski M 2006. Geochronology of the crystalline basement of the Western Outer Carpathians' source areas — constraints from the K/Ar dating of mica and Th–U–Pb chemical dating of monazite from the crystalline ‘exotic’ pebbles. Geolines 20: 110–112.

  • Poprawa P and Malata T 2006. Model of Late Jurassic to Early Miocene tectonic evolution of the Western Outer Carpathians. Przegląd Geologiczny 54: 1066–1080 (in Polish).

  • Pupin JP 1980. Zircon and Granite Petrology. Contributions to Mineralogy and Petrology 73: 207–220 DOI 10.1007/BF00381441.

    • Crossref
    • Export Citation
  • Salata D and Oszczypko N 2010. Preliminary results of provenance analyses of exotic magmatic and metamorphic rock pebbles from the Eocene flysch deposits of the Magura Nappe (Krynica facies zone Polish Outer Carpathians). In: Christofidis G Kantiranis N Kostopoulos DN and Chatzipetros AA eds. Proceedings of the XIX CBGA Congress Thessaloniki Greece Scientific Annals School of Geology Aristotle University of Thessaloniki special volume 100: 241–249.

  • Sikora WJ 1976. Kordyliery Karpat Zachodnich w świetle tektoniki płyt litosfery (Cordilleres of the Western Carpathians in the light of the plate tectonics theory). Przegląd Geologiczny 6: 336–349 (in Polish).

  • Sláma J Košler J Condon DJ Crowley JL Gerdes A Hanchar JM. Horstwood MSW Morris GA Nasdala L Norberg N Schaltegger U Schoene B Tubrett MN and Whitehouse MJ 2008. Plešovice zircon – a new natural reference material for U-Pb and Hf isotopic microanalysis. Chemical Geology 249: 1–35 DOI 10.1016/j.chemgeo.2007.11.005.

    • Crossref
    • Export Citation
  • Ślączka A 1986. Europejskie spotkania sedymentologów (European sedimentologists' meetings). Przegląd Geologiczny 34(4): 231.

  • Ślączka A and Kaminski MA 1998. A Guidebook to Excursions in the Polish Flysch Carpathians. Grzybowski Foundation Special Publication 6: 171 pp.

  • Ślączka A Krugłov S Golonka J Oszczypko N and Popadyuk I 2006. Geology and Hydrocarbon Resources of the Outer Carpathians Poland Slovakia and Ukraine: General Geology. In: Golonka J and Picha FJ eds. The Carpathians and their foreland: Geology and hydrocarbon resources. AAPG Memoir 84: 221–259.

  • Sun SS and McDonough WF 1989. Chemical and isotopical systematics of oceanic basalts: implications for mantle composition and processes. Magmatism in the Oceanic Basins. Geological Society of London Special Pubplications 42: 313–345.

    • Crossref
    • Export Citation
  • Sylvester PJ and Ghaderi M 1997. Trace element analysis of scheelite by excimer laser ablation-inductively coupled plasma-mass spectrometry (ELA-ICP-MS) using a synthetic silicate glass standard. Chemical Geology 141: 49–65 DOI 10.1016/S0009-2541(97)00057-0.

    • Crossref
    • Export Citation
  • Thöni M Miller C Zanetti A Habler G and Goessler W 2008. Sm–Nd isotope systematics of high-REE accessory minerals and major phases: ID-TIMS LA-ICPMS and EPMA data constrain multiple Permian-Triassic pegmatite emplacement in the Koralpe Eastern Alps. Chemical Geology 254: 216–237 DOI 10.1016/j.chemgeo.2008.03.008.

    • Crossref
    • Export Citation
  • Unrug R 1963. Istebna beds - a fluxoturbidity formation in the Carpathian Flysch. Rocznik Polskiego Towarzystwa Geologicznego 33: 49–92.

  • Unrug R 1968. Kordyliera śląska jako obszar źródłowy materiału klastycznego piaskowców fliszowych Beskidu Śląskiego i Beskidu Wysokiego (Polskie Karpaty zachodnie) (The Silesian cordillera as the source of clastic material of the Flysch sandstones of the Beskid Śląski and Beskid Wysoki ranges (Polish Western Carpathians). Rocznik Polskiego Towarzystwa Geologicznego 38: 81– 164.

  • Watson TM and Harrison EB 1983. Zircon saturation revisited: temperature and composition effects in a variety of crustal magma types. Earth and Planetary Science Letters 64: 295–304 DOI 10.1016/0012-821X(83)90211-X.

    • Crossref
    • Export Citation
  • Wieser T 1948. Crystalline exotic blocks in the Silesian Cretaceous of the Wadowice area (Pl. I-II). Annales Societatis Geologorum Poloniae 18: 36–150 (in Polish).

  • Wieser T 1949. Egzotyki krystaliczne w kredzie śląskiej okolic Wadowic (Crystalline exotic blocks in the Silesian Cretaceous of the Wadowice area). Rocznik Polskiego Towarzystwa Geologicznego 18: 36–105 (in Polish).

  • Wieser T 1985. Some remarks on the sedimentation composition and provenance of exotic bearing conglomerates in the western Polish Carpathians Flysch formations. 13th Congress Carpatho-Balkan Geological Association Guide 1. Geological Institute Kraków: 57–68.

  • Żelaźniewicz A Buła Z Fanning M Seghedi A and Żaba J 2009. More evidence on Neoproterozoic terranes in Southern Poland and south eastern Romania. Geological Quarterly 58(1): 93–124.

  • Żelaźniewicz A Aleksandrowski P Buła Z Karnkowski PH Konon A Oszczypko N Ślączka A Żaba J and Żytko K 2011. Regionalizacja tektoniczna Polski (Tectonic regionalization of Poland). Komitet Nauk Geologicznych PAN Wrocław: 59 pp (in Polish).

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Figures
  • View in gallery

    Simplified geological map of the Polish part of the Western Carpathians (after Żelaźniewicz el al., 2011, modified) with the location of the investigated samples (shown as yellow dots).

  • View in gallery

    Field photo (a) of the Bugaj granitoid (sample Bu1) and field photo (b) of the Andrychów orthogneiss (sample An).

  • View in gallery

    Classification position of the Bugaj granitoids in: (a) alkali (K2O + Na2O) versus SiO2 (TAS) classification diagram (Middlemost, 1985); (b) Primitive mantle-normalized (Sun and McDonough, 1989) multielement “spider” diagrams; (c) classification position of the Bugaj granitoids in Multicationic R1–R2 diagram (De La Roche et al.,1980), with fields numbered according to Batchelor and Bowden (1985); 1 – mantle fractionates, 2 – pre-plate collision suites, 3 – post-collision suites, 4 – late orogenic magmas, 5 – anorogenic suites, 6 – syncollisional (anatectic) suites. R1 = 4Si − 11(Na + K) − 2(Fe + Ti); R2 = 6Ca + 2 Mg + Al.

  • View in gallery

    Secondary electron (SE) images of selected zircon crystals from granite sample Bu1. See text for description.

  • View in gallery

    Compiled cathodoluminescence (CL) images showing the range of textures observed in zircon crystals from granite sample Bu1. See text for details. The white rectangles show the approximate location of laser ablation trenches (confirmed by re-inspecting grains under CL after the LA analysis) and are not to scale. The numbers refer to the analytical data presented in Table 3.

  • View in gallery

    Tera-Wasserburg diagrams presenting the U/Pb age of the zircons from granite sample Bu1: a) all data points; b) concordant to sub-concordant data points. The inherited xenocryst (p2Bu_23) and the three data points showing recent lead loss (p3Bu_01/1, p3Bu_01/1, p3Bu_09/1) are not shown.

  • View in gallery

    Secondary electron (SE) images of selected zircon crystals from orthogneiss sample An. See text for description.

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    Compiled cathodoluminescence (CL) images showing the range of textures observed in zircon crystals from orthogneiss sample An. See text for details. The white rectangles show the approximate location of laser ablation trenches (confirmed by re-inspecting grains under CL after the LA analysis) and are not to scale. The numbers refer to the analytical data presented in Table 3.

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    Tera-Wasserburg diagrams for isotopic ratio for zircon crystals from orthogneiss sample An: a) all data points; b) concordant to sub-concordant data points defining a discordia line with a lower intercept of 542 ± 21 Ma (forced through data point p3An_06/1). The inherited xenocrysts (p3An_06/1, p3An_06/2) and the two data points showing recent lead loss (p3An_08, p3An_13) are not shown.

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