Characterization of Nanometric-Sized Carbides Formed During Tempering of Carbide-Steel Cermets

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Abstract

The aim of this article of this paper is to present issues related to characterization of nanometric-sized carbides, nitrides and/or carbonitrides formed during tempering of carbide-steel cermets. Closer examination of those materials is important because of hardness growth of carbide-steel cermet after tempering. The results obtained during research show that the upswing of hardness is significantly higher than for high-speed steels. Another interesting fact is the displacement of secondary hardness effect observed for this material to a higher tempering temperature range. Determined influence of the atmosphere in the sintering process on precipitations formed during tempering of carbide-steel cermets. So far examination of carbidesteel cermet produced by powder injection moulding was carried out mainly in the scanning electron microscope. A proper description of nanosized particles is both important and difficult as achievements of nanoscience and nanotechnology confirm the significant influence of nanocrystalline particles on material properties even if its mass fraction is undetectable by standard methods. The following research studies have been carried out using transmission electron microscopy, mainly selected area electron diffraction and energy dispersive spectroscopy. The obtained results and computer simulations comparison were made.

[1] G. Matula, L.A. Dobrzański, A. Várez, B. Levenfeld, J.M. Torralba, J Mater Process Tech. 162, 230-235 (2005).

[2] M. Bonek, G. Matula, L.A. Dobrzański, Adv Mat Res. 291-294, 1365-1268 (2011).

[3] L.A. Dobrzański, D. Pakuła, J. Mikuła, K. Gołombek, Int. J Surf Sci Eng, 1, (1), 111-124 (2007).

[4] P. Echlin, Springer, Handbook of sample preparation for scanning electron microscopy and x-ray microanalysis, New York 2009.

[5] L.A. Dobrzański , K. Gołombek, J Mater Process Tech, 164-165, 805-815 (2005).

[6] S. Kuimalee, T. Chairuangsri, J.T.H. Pearce, D.V. Edmonds, A.P. Brown, R.M.D. Brydson, Micron 41, (5), 423-429 (2010).

[7] P.W. Hawkes, J.C.H Spence, Springer, Science of microscopy, New York 2007.

[8] J.A. Pérez-Omil. PhD thesis, University of Cadiz-Spain (1994).

[9] S. Bernal, F.J. Botana, J.J. Calvino, C. Lopez-Cartes, J.A. Perez-Omil, J.M. Rodriguez-Izquierdo. Ultramicroscopy 72, 135-164 (1998).

Archives of Metallurgy and Materials

The Journal of Institute of Metallurgy and Materials Science and Commitee on Metallurgy of Polish Academy of Sciences

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