Influence of relevant parameters on the extraction efficiency and the stability of the microdrop in the single drop microextraction

Open access


Single drop microextraction technique uses microamounts of organic solvents. Simplicity, low cost, low environmental impact, compatibility with chromatographic systems as well as its applicability to different matrices are main advantages of single drop microextraction. This technique has become frequently used for the extraction of a broad scope of compounds for numerous analytical applications. This review provides an overview of the existing single drop microextraction modes of realisation and the main scope is devoted to the optimization of parameters influencing the efficiency. The state of the art is discussed on the basis of examples selected from representative application areas. Extraction parameters for toxic organic compounds extraction and microdrop stability were evaluated.

Andraščíková M, Matisová E, Hrouzková S (2015) Separation and Purification Reviews 44: 1-18.

Andruch V, Kocúrová L, Balogh IS, Škrlíková J (2012) Microchemical Journal 102: 1-10.

Amde M, Tan ZQ, Liu R, Liu JF (2015) Journal of Chromatography A 1395: 17-15.

Amvrazi EG, Tsiropoulos NG (2009) Journal of Chromatography A 1216: 2789-2797.

Asensio-Ramos M, Ravelo-Pérez LM, González-Curbelo MÁ, Hernández-Borges J (2011) Journal of Chromatography A 1218: 7415-7437.

Carlos EA, Alves RD, de Queiroz MERL, Neves AA (2013) Journal of Brazilian Chemical Society 24: 1217-1227.

Cortada C, Vidal L, Tejada S, Romo A (2009) Analytica Chimica Acta 638: 29-35.

Garbi A, Sakkas V, Fiamegos YC, Stalikas CD, Albanis T (2010) Talanta 82: 1286-1291.

Hrouzková S (2017) In: “Food analysis: Innovative analytical tools for safety and quality assessment”, Umile Gianfranco Spizzirri, Giuseppe Cirillo (Ed), John Wiley &Sons, Hoboken, New Jersey and Scrivener Publishing, Beverly, MA, 2017, p. 221.

Hrouzková S, Szarka A, Zichová S (2018) Chemické listy 112: 165-174.

Jain A, Verma KK (2011) Analytica Chimica Acta 706: 37-65.

Jeannot MA, Cantwell FF (1996) Analytical Chemistry 69: 2236-2240.

Jeannot MA, Cantwell FF (1997) Analytical Chemistry 69: 235-239.

Jeannot MA, Przyjazny A, Kokosa JM (2010) Journal of Chromatography A 1217: 2326-2336.

Kokosa JM (2015) Trends in Analytical Chemistry 71: 194-204.

Liu W, Lee HK (2000) Analitical Chemistry 72: 4462-4467.

Mingyuan G, Yangcheng L, Guangsheng L (2009) Analytica Chimica Acta 648: 123-127.

Pena-Pereira F, Lavilla I, Bendicho C (2010) Trends in Analytical Chemistry 29: 617-628.

Perreira dos Anjos J, de Andrade JB (2014) Microchemical Journal 112: 119-126.

Perreira dos Anjos J, de Andrade JB (2015) Microchemical Journal 120: 69-76.

Płotka-Wasylka J, Owczarek K, Namieśnik J (2016) Trends in Analytical Chemistry 85: 46-64.

Psillakis E, Kalogerakis N (2001) Journal of Chromatography A 938: 113-120.

Psillakis E, Kalogerakis N (2002) Trends in Analytical Chemistry 2: 53-63.

Salemi A, Rasoolzadeh R, Nejad MM, Vosough M (2013) Analytica Chimica Acta 769: 121-126.

Sarafraz-Yazdi A, Amiri A (2010) Trends in Analytical Chemistry 29: 1-14.

Tobiszewski M, Mechlinska A, Zygmunt B, Namiesnik J (2009) Trends in Analytical Chemistry 28: 943-951.

Vidal L, Canals A, Kalogerakis N, Psillakis E (2005) Journal of Chromatography A 1089: 25-30.

Wang X, Ying L, Cai F, Qing Q, Yuan K, Chen B, Luan T (2017) Talanta 164: 727-734.

Wu L, Hu M, Li Z, Song Y, Cui Y, Zhang H, Yu A, Ma Q, Wang Z (2016) Food Chemistry 192: 596-602.

Wu L, Hu M, Li Z, Song Y, Zhang H, Yu A, Ma Q, Wang Z (2015) Journal of Chromatography A 1407: 42-51.

Yangcheng L, Quan L, Guangsheng L, Youyuan D (2006) Analytica Chimica Acta 566: 259-264.

Ye C, Zhou Q, Wang X (2007) Journal of Chromatography A 1139: 7-13.

Yohannes A, Tolesa T, Merdassa Y, Megersa (2016) Journal of Analytical and Bioanaltical Technology 7: 1-8.

Xia L, Hu B, Jiang Z, Wu Y, Li L, Chen R (2005) Journal of Analytical Atomic Spectrometry 20: 441-446.

Xu L, Basheer Ch, Lee HK (2007) Journal of Chromatography A 1152: 184-192.

Zhao E, an L, Jiang S, Wang Q, Zhou Z (2006) Journal of Chromatography A 1114: 269-273.

Acta Chimica Slovaca

The Journal of Slovak University of Technology in Bratislava

Journal Information


All Time Past Year Past 30 Days
Abstract Views 0 0 0
Full Text Views 172 172 18
PDF Downloads 75 75 14