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REFERENCES [1] B alachowski L., S ikora Z., Mechanical properties of bottom ash – dredged material mixtures in laboratory tests , Studia Geotechnica et Mechanica, 2013, Vol. 35, No. 3. [2] C antré S. et al., Full-Scale Flume Experiments to Analyse the Surface Erosion Resistance of Dike Embankments Made of Dredged Materials , ASCE Journal of Waterway, Port, Coastal and Ocean Engineering, published online January 2017, http://dx.doi.org/10.1061/(ASCE)WW.1943-5460.0000375 . [3] C antré S., S aathoff F., Installation of fine-grained organic dredged materials

Abstract

The hydrothermal synthesis of MCM-22 zeolite was carried out using silica, sodium aluminate and hexamethyleneimine, under static conditions at 150 °C for a period of 10 days, followed by washing with deionized water, drying overnight and calcination at 650 °C. The obtained material was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and scanning electron microscopy (SEM). The XRD analysis evidenced that MCM-22 presented a well defined MWW structure. The FT-IR spectrum confirmed the efficiency of the hexamethyleneimine as an organic template used to direct the structure of the MCM-22 zeolite under static conditions. The SEM image indicated that the particles are spherical in shape, with a diameter of ca. 10 μm. The acid properties of the MCM-22 zeolite, as determined by n-buthylamine adsorption, were investigated in the temperature ranges of 105 to 300 °C and 300 to 525 °C, relative to medium and strong acid sites, respectively.

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