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References Abbood A, Aldiab D (2017) HPLC determination of caffeine in some beverages and pharmaceutical dosage forms available in Syrian market. J. Chem. Pharm. Sci. 10: 1174-1179. Bae IK, Ham HM, Jeong MH, Kim DH, Kim HJ (2015) Simultaneous determination of 15 phenolic compounds and caffeine in teas and mate using RP-HPLC/UV detection: Method development and optimization of extraction process. Food Chem. 172: 469-475. de Mejia EG, Ramirez-mares MV (2014) Impact of caffeine and coffee on our health. Trends Endocrinol. Metab. 25: 489-492. Gibson CM, Fowler PW

, 2008. 5. Zatonski W. et al.: An uncontrolled trial of cytisine (Tabex) for smoking cessation. Tob Control., 15, 481, 2006. 6. Coe J.W. et al.: Varenicline: an alpha4beta2 nicotinic receptor partial agonist for smoking cessation. J Med Chem., 48, 3474, 2005. 7. Balaji M. et al.: Development and validation of related substances method for Varenicline and its impurities. Der Pharmacia Lettre., 8, 304, 2016. 8. Pujeri S.S., Khader A.M., Seetharamappa J.: Stress degradation studies on varenicline tartrate and development of a validated stability-indicating HPLC method

of HPLC method for the determination of S (-) Amlodipine Besylate and its related substance in tablet formulation by using chiral separation. Asian J Biomed Pharm Sci. 2012;2(12):60-64. 10. Zandkarimi M, Shafaati A, Foroutan SM, Lucy CA - Rapid enantioseparation of amlodipine by highly sulfated cyclodextrins using short-end injection capillary electrophoresis. DARU. 2009;17(4):269-275. 11. Owens PK, Fell AF, Coleman MW, Berridge JC - Effect of charged and uncharged chiral additives on the resolution of amlodipine enantiomers in liquid chromatography and capillary

.12.004. 25. Tsaknis J, Lalas S, Evmorfopoulos E. Determination of malondialdehyde in traditional fish products by HPLC. Analyst. 1999 Jun;124(6):843-5. DOI: 10.1039/ a902026h. 26. Siddique YH, Ara G, Afzal M. Estimation of lipid peroxidation induced by hydrogen peroxide in cultured human lymphocytes. Dose Response. 2012;10(1):1-10. DOI: 10.2203/dose-response.10-002.Siddique. 27. Khalili J, Biloklytska HF. Salivary malondialdehyde levels in clinically healthy and periodontal diseased individuals. Oral Dis. 2008 Nov;14(8):754-60. DOI: 10.1111/j.1601-0825.2008.01464.x. 28

References 1. Semenkin AA, Zhenatov AB, Zhivilova LA et al. Comparative evaluation of vascular and metabolic effects of perindopril combination with indapamide-retard or hydrochlorothiazide in hypertensive patients. Artery Res. 2011;5:188. 2. Roux A, Lison D, Junot C et al. Applications of liquid chromatography coupled to mass spectrometry-based metabolomics in clinical chemistry and toxicology: A review. Clin Biochem. 2011;44:119-135. 3. Simonic Z, Roskar R, Gartner A, et al. The use of microcalorimetry and HPLC for the determination of degradation kinetics and

;12:614-20. Bhushan R, Arora M. Direct enantiomeric resolution of (±) atenolol, (±) metoprolol, and (±) propranolol by impregnated TLC using L-aspartic acid as chiral selector. Biomed Chrom. 2003;17:226-230. Bhushan R, Tanwar S. Direct TLC resolution of atenolol and propranolol into their enantiomers using different chiral selectors as impregnating reagents. Biomed Chrom. 2008;22:1028-1034. Bruchata K, Čižmarikova R, Polakovičova M, Hroboňova K, Pastirova Z. Synthesis, conformational study and HPLC enantioseparation of nitrophenoxyaminopropanols. Acta Facult Pharm Univ

Union L 342: 59. Hroboňová K, Lehotay J, Čižmárik J, Sádecká J (2013) Comparison HPLC and fluorescence spectrometry methods for determination of coumarinn derivatives in propolis. J. Liq. Chromatogr. Relat. Technol. 36: 486-503. Ikeda R, Wada M, Nishigaki T, Nakashima K (2009) Quantitation of coumarin derivatives in Noni ( Morinda citrifilia ) and their contribution of guenching effect on reactive oxygen species. Food Chem. 113: 1169-1172. Marcolan M, Martins PA, Pedrosa VA, Rodrigues RH, De Oliveira HPM, Codognoto L (2011) Spectrofluorimetric determination of

simultaneous dual wavelength UV-HPLC method for the determination of potential impurities in fampridine active pharmaceutical ingredient, J. Pharm. Biomed. Anal. 58 (2012) 136–140; https://doi.org/10.1016/j.jpba.2011.09.009 11. C. Babu, K. N. Rao, N. Devanna and K. S Reddy, Development and validation of stability indicating reversed phase high performance liquid chromatographic method for the determination of related substances in fampridine drug substance and tablet dosage forms, Asian J. Pharm. Clin. Res . 10 (2017) 334–338. 12. N. R. Dharani, K. Padmini and S

References The Merck Index , 13th ed., Merck White House Station, 2001, p. 1452. Y. Jin, Determination of related substances in raloxifene hydrochloride raw medicine by HPLC, Huaxue Gongye Yu Gongcheng Jishu 25 (2004) 56-57; ref. Chem. Abstr. 144 (2005) 135501. J. Trontelj, T. Vovic, M. Bogataj and A. Mrhar, HPLC analysis of raloxifene hydrochloride and its application to drug quality control studies, Pharm. Res. 52 (2005) 334-339. Q. Wang, H. Zhang and Z. Yu, Determination of the content of raloxifene hydrochloride by HPLC, Shenyang Yaoke Daxue Xuebao 19

and F. Tomas, An HPLC study of flavones from some Spanish Sideritis species, Phytochemistry 24 (1985) 1285--1288. F. A. T. Barberan, M. I. Gil, F. Ferreres, D. Rivera, C. Obon and F. T. Lorente, Distribution of 8-hydroxyflavone glycosides and flavonoid aglycones in some Spanish Sideritis species, Biochem. Syst. Ecol. 21 (1993) 487--497. O. M. Palomino, P. Gomez-Serranillos, E. Carretero and A. Villar, High-performance liquid chromatography of flavonoids from Sideritis species, J. Chromatogr. A 731 (1996) 103--108. M. I. Gil, F. Ferreres, A. Marrero, F. T