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Krystyna Pohorecka, Tomasz Kiljanek, Maja Antczak, Piotr Skubida, Piotr Semkiw and Andrzej Posyniak

treatment of honeybee colonies with Apiwarol by smouldering tablet directly in hives, residues of DMF, DMPF, and 2,4-DMA in centrifuged honey reached mean levels of 2.3 μg/kg (from 1.9 to 2.6 μg/kg), 2.4 μg/kg (from 1.9 to 2.9 μg/kg), and 84.9 μg/kg (from 68.6 to 98.4 μg/kg), respectively. Table 1 The amitraz metabolite profile in honey samples, separately presented for each group Group W – Apiwarol combustion in Wakont (n = 27) Group B – Apiwarol combustion in hive (n = 27) Concentration (μg/kg) Concentration (μg/kg) Metabolite

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Robert Gąsior, Marta Szczypuła and Zbigniew Szybiński

-induced combustion. Anal. Bio anal. Chem., 398: 1125-1131. Souzade S.V.C., Pinto C.T., Junqueira R.G. (2007). In-house method validation: Application in arsenic analysis. J. Food Comp. Anal., 20, 3-4: 241-247. Szybiński Z., Jarosz M., Hubalewska-Dedejczyk A., Stolarz-Skrzypek K., Kawecka-Jaszcz K., Traczyk I., Stoś K. (2009). Iodine-deficiency prophylaxis and the restriction of salt consumption -a21st century challenge. Pol. J. Endocrinol., 61: 135-140. Szybiński Z., Lewi ński A. (1998). National programme for the elimination of

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Iwona Matraszek-Żuchowska, Barbara Woźniak, Alicja Kłopot, Sebastian Witek, Katarzyna Sielska and Andrzej Posyniak

Weter 2010, 66, 177–181. 35. Yamada M., Kinoshita K., Kurosawa M., Saito K., Nakazawa H.: Analysis of exogenous nandrolone metabolite in horse urine by gas chromatography/combustion/carbon isotope ratio mass spectrometry. J Pharm Biomed Anal 2007, 45, 654–658.