The aim of this study was to investigate the usage of Dynamic Image Analysis for determination of size, shape and distribution of granules of microcrystalline cellulose, created by high shear granulation. A series of experiments was carried out to analyse the effect of process parameters on a created granule morphology. The amount of the granulation liquid and speed of the impeller have a significant effect on the median size granule value, the sphericity, the granule distribution width, but also on the granulation process yield.
Selective adjustment of the properties of particular material agglomeration has its inherent place in the chemical, food, but especially in the pharmaceutical, industry. The requirement to produce an agglomerate with desired particle size at a given strength is often formulated. To create the targeted product, it is necessary to know the process parameters affecting the preparation of its features. This paper deals with survey distribution characteristics and compressibility changes of an agglomerate in dependence on the duration of the granulation process through the usage of the most modern devices working with particulate materials. The investigated product will be prepared for coating granulating disc designed at the Institute of Process Engineering, Faculty of Mechanical Engineering, Slovak University of Technology in Bratislava.
Calcium carbonate in the form of finely ground limestone is a material that has found its application in a wide range of industries, in the chemical, rubber, agricultural, and paper industries, is used for desulfurization of boilers and other. In civil engineering, ground limestone is used for the production of building materials, plaster and mortar mixtures, as a filler in concrete mixtures, in road construction, and as an essential component of mastic asphalt. This paper deals with examining the modification of the properties of finely ground limestone by the tumbling agglomeration method. It has been shown that the components of concrete with a round grain have a positive effect on the pumping of concrete in comparison with an elongated grain or the rough surface of crushed stone. The experiments will be carried out on a granulation plate using a variety of granulation liquid. The agglomerates and their properties were compared with untreated finely ground limestone, with a focus on detecting changes in compressibility, density and particle size. The output of this paper is a description and graphical representation of the changes in the properties of ground limestone before and after the agglomeration process.