Influence of Direct Thermal Analysis Experimental Conditions on Determination of the High Temperature Phase Transformation Temperatures / Wpływ Warunków Prowadzenia Bezpośredniej Analizy Termicznej Na Określenie Temperatur Wysoko Temperaturowych Przemian Fazowych

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Thermo-physical and thermodynamic properties of metallic systems represent some of the most important data that allows to describe their behaviour under strictly specified conditions. These data are the basic, input data for simulative programs, which can model this behaviour and they can be applied to real conditions. Method of direct thermal analysis is the one of the methods of enabling to obtain such data. This paper deals with application of this method on particular sample of pure standard material. The experimental laboratory system for thermal analysis Netzsch STA 449 F3 Jupiter was used for experimental measurements. This paper is studying the influence of experimental conditions on the obtained temperature of phase transformations and on shift of phase transformation temperatures with respect to the monitored experimental conditions, accuracy and credibility of the measured data. Acquired values of this data could be significantly influenced by experimental conditions, size (mass) of samples, purity of inert atmosphere and also by regimes of controlled heating and cooling rates.

[1] P.K. Gallagher, Handbook of Thermal Analysis and Calorimetry: Principles and Practice. 1. First edition 1998. Second impression, Amsterdam: Elsevier Science B.V., 2003.

[2] E. Gmelin, S.M. Sarge, Thermochimica Acta 347, 9-13 (2000).

[3] S.M. Sarge, G.W.H. Hohne, H.K. Camenga, W. Eysel, E. Gmelin, Thermochimica Acta 361, 1-20 (2000).

[4] W.J. Boettinger, U.R. Kattner, K.-W. Moon, National institute of standards and technology. DTA and Heatflux DSC Measurements of Alloy Melting and Freezing: NIST Recommended Practice Guide. Spec. Publ. 960-15. Washington: U.S. Government printing office, 2006.

[5] K. Gryc, B. Smetana, M. Zaludova, K. Michalek, M. Tkadleckova, J. Dobrovska, L. Socha, L. Valek, R. Pachlopnik, Metalurgia 52 (4), 445-448 (2013).

Archives of Metallurgy and Materials

The Journal of Institute of Metallurgy and Materials Science and Commitee on Metallurgy of Polish Academy of Sciences

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