Electrochemical Synthesis of ZnO Nanoparticles During Anodic Dissolution of Zinc in Alcohols Solvents

Open access

Electrochemical Synthesis of ZnO Nanoparticles During Anodic Dissolution of Zinc in Alcohols Solvents

Studies of the effect of the kind of alcohol, electrolyte concentration and water on the anodic dissolution of zinc and the nature of dissolution products were performed. The dissolution products were analyzed by spectroscopic methods (SEM/EDS, XPS and UV-vis) and X-ray diffraction. These studies have shown that the process of anodic dissolution of zinc in alcohol electrolytes (methanol and ethanol) in the presence of water (1-5% vol.), is a simple way to obtain ZnO nanoparticles.

R. Viswanathan, R. B. Gupta, The Journal of Supercritical Fluids 27, 187 (2003).

B. Baruwati, D. K. Kumar, S. V. Manorama, Sensors and Actuators B 119, 676 (2006).

S. Musić, D. Dragćević, S. Popović, M. Invanda, Materials Letters 59, 2388 (2005).

R. Wu, C. S. Xie, H. Xia, J. H. Hu, A. H. Wang, Journal of Crystal Growth 217, 274 (2000).

K. G. Kanade, B. B. Kale, R. C. Aiyer, B. K. Das, Materials Research Bulletin 41, 590 (2006).

L. Poul, S. Ammar, N. Jouini, F. Fievet, F. Villain, Journal of Sol-Gel Science and Technology 26, 261 (2003).

E. J. Hosono, S. Fujihara, T. Kimura, H. Imai, Journal of Sol-Gel Science and Technology 29, 1528 (2004).

Chin-Hsien Hung, Wha-Tzong Whang, Materials Chemistry and Physics 82, 705 (2003).

H. Wang, CH. Xie, D. Zeng, Journal of Crystal Growth 277, 372 (2005).

G. S. Huang, X. L. Wu, Y. C. Cheng, J. C. Shen, A. P. Huang, P. K. Chu, Applied Physics A 86, 463 (2007).

K. L. Levine, J. O. Iroh, P. B. Kosel, Applied Surface Science 24, 230 (2004).

H. Li, R. Wang, Ch. Guo, H. Zhang, Materials Science and Engineering B 103, 285 (2003).

G. Zhao, J.-J. Xu, H.-Y. Chen, Analytical Biochemistry 350, 145 (2006).

Y.-F. Gao, M. Nagai, Y. Masuda, F. Sato, K. Koumoto, Journal of Crystal Growth 286, 445 (2006).

B. Stypula, J. Banas, T. Habdank-Wojewódzki, H. Krawiec, M. Starowicz, PATENT: P-369 320 Sposób otrzymywania mikro- i nanoczastek tlenków metali, reported: 28.07.2004, grantem: 07.10.2009.

M. Starowicz, B. Stypuła, European Journal of Inorganic Chemistry 6, 872 (2008).

B. Stypuła, M. Starowicz, D. Kasprzyk, M. Hajos, Ochrona Przed Korozją 11, 551 (2009).

S. Białłozor, E. T. Bandura, Electrochim. Acta 37, 891 (1987).

U. Lechner-Knoblauch, E. Heitz, Electrochim. Acta 32, 901 (1987).

X. G. Zhang, Corrosion and Electrochemistry of Zinc: Plenum Press, New York, (1996).

J. Światowska-Mrowiecka, J. Banaś, Electrochim. Acta 50, 1829 (2005).

J. Banaś, K. G. Schütze, E. Heitz, J. Electrochem. Soc. 133, 253 (1986).

J. Banaś, B. Stypuła, K. Banaś, J. Światowska-Mrowiecka, M. Starowicz, U. Lelek-Borkowska, Journal of Solid State Electrochemistry 13, 1669 (2009).

C. D. Wagner, J. F. Moulder, L. E. Davis, W. M. Riggs, Handbook of X-ray photoelectron spectroscopy, Perking-Elmer Corporation Physical Electronics Division (end of book), (1995).

J. G. Dillard, L. T. Taylor, R. D. Seals, R. Alexander, Inorganic Chemistry 12, 2485 (1973).

G. Haemers, J. J. Verbist, S. Maroie, Applications of Surface Science 17, 463 (1984).

A. M. Beccaria, G. Castello, G. Poggi, British Corrosion Journal 30, 283 (1995).

K. Merritt, R. S. Wortman, M. Millard, S. A. Brown, Biomat. Med. Dev. Art. Org. 11, 115 (1983).

J. M. Kołotyrkin, Elektrochimia mietałow w niewodnych raztworach, Mir, Moskwa (1974).

Archives of Metallurgy and Materials

The Journal of Institute of Metallurgy and Materials Science and Commitee on Metallurgy of Polish Academy of Sciences

Journal Information

IMPACT FACTOR 2016: 0.571
5-year IMPACT FACTOR: 0.776

CiteScore 2016: 0.85

SCImago Journal Rank (SJR) 2016: 0.347
Source Normalized Impact per Paper (SNIP) 2016: 0.740

Cited By


All Time Past Year Past 30 Days
Abstract Views 0 0 0
Full Text Views 166 165 13
PDF Downloads 88 87 5